2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester

Base Information

• Chemical Name: 2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester
• CAS No.: 1027075-64-4
• Molecular Formula: C₁₉H₁₈O₅
• Molecular Weight: 326.349
• Mol file: 1027075-64-4.mol

Synonyms:2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester

Chemical Property of 2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester

There total 1 articles about 2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

C19H22O3 (1027075-70-2) → 2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester (1027075-64-4)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetic acid; at 20 ℃;

DOI:10.1016/j.bmcl.2008.02.082

Reference yield: 39.0%

2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester (1027075-64-4) + 2',4'-dimethoxyacetophenone (829-20-9) → C39H42O11 (1027075-78-0)

Guidance literature:

2',4'-dimethoxyacetophenone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester; In tetrahydrofuran; hexane; at -78 - 0 ℃; Further stages.;

DOI:10.1016/j.bmcl.2008.02.082

Reference yield:

2,2-dimethyl-propionic acid 5-formyl-2-(4-formyl-phenoxy)-phenyl ester (1027075-64-4) + ethyl (triphenylphosphoranylidene)acetate (1099-45-2) → C27H30O7

Guidance literature:

With potassium carbonate; In 1,4-dioxane; chloroform; at 110 ℃; for 18h;

DOI:10.1016/j.bmcl.2008.02.082

upstream raw materials:

C₁₉H₂₂O₃

Downstream raw materials:

C₃₉H₄₂O₁₁