Technology Process of C25H34O7S
There total 3 articles about C25H34O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium cyanotrihydroborate; trifluoroacetic acid;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 6h;
Molecular sieve;
DOI:10.1016/j.bmcl.2011.03.064
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / acetonitrile / 2 h / 20 °C
2.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
2.2: 6 h / 80 °C
3.1: sodium cyanotrihydroborate; trifluoroacetic acid / N,N-dimethyl-formamide / 6 h / 0 °C / Molecular sieve
With
sodium cyanotrihydroborate; di(n-butyl)tin oxide; toluene-4-sulfonic acid; trifluoroacetic acid;
In
methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.03.064
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
1.2: 6 h / 80 °C
2.1: sodium cyanotrihydroborate; trifluoroacetic acid / N,N-dimethyl-formamide / 6 h / 0 °C / Molecular sieve
With
sodium cyanotrihydroborate; di(n-butyl)tin oxide; trifluoroacetic acid;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.064