1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane

Base Information

• Chemical Name: 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane
• CAS No.: 892393-27-0
• Molecular Formula: C₁₆H₂₁N₃O₂
• Molecular Weight: 287.362

Synonyms:1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane

Chemical Property of 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane

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Technology Process of 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane

There total 1 articles about 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H21N3O2*C19H15Cl + C16H21N3O2*C19H15Cl → 1-(5-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane (892393-28-1) + 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane (892393-27-0)

Guidance literature:

In methanol; at 80 ℃; for 4h; Product distribution / selectivity; Heating / reflux;

Reference yield: 87.0%

1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane (892393-27-0) → 1-(3-aminophenyl)-1-(4-methyl-1H-imidazol-1-yl)methane (892393-25-8)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; methanol; at 25 ℃; for 5h;

Reference yield:

1-(5-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane (892393-28-1) + 1-(4-methyl-1H-imidazol-1-yl)-1-[3-[(tert-butoxycarbonyl)-amino]phenyl]methane (892393-27-0) + trityl chloride (76-83-5) → C16H21N3O2*C19H15Cl + C16H21N3O2*C19H15Cl

Guidance literature:

In dichloromethane; at 0 ℃; for 2h;

Downstream raw materials:

1-(3-aminophenyl)-1-(4-methyl-1H-imidazol-1-yl)methane

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