C₃₉H₆₈O₇Si₂

Base Information

Chemical Name:C₃₉H₆₈O₇Si₂
CAS No.:1335098-51-5
Molecular Formula:C₃₉H₆₈O₇Si₂
Molecular Weight:705.136
Hs Code.:

C<sub>39</sub>H<sub>68</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₃₉H₆₈O₇Si₂

Suppliers and Price of C₃₉H₆₈O₇Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₆₈O₇Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₆₈O₇Si₂

There total 6 articles about C₃₉H₆₈O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942505-83-1
(2S,6R)-2-[(2R,4R,6R,7S)-2,4-bis-(tert-butyl-dimethylsilanyloxy)-6-(4-methoxybenzyloxy)-7-methylnon-8-ynyl]-6-[2-(tert-butyl-dimethylsilanyloxy)ethyl]tetrahydropyran

: 1335098-51-5
C₃₉H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 6-(2,4,6-triphenyl-phenyl)-2-diphenylphosphino-pyridine; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate / water; acetone / 21.5 h / 60 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 14 h / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 - 0 °C / Inert atmosphere

3.2: 2 h / -78 °C / Inert atmosphere

4.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 14 h / -10 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / Inert atmosphere

With pyridine; 6-(2,4,6-triphenyl-phenyl)-2-diphenylphosphino-pyridine; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1002/anie.201103270

Reference yield:

: 1335098-25-3
C₄₅H₈₄O₆Si₃

: 1335098-51-5
C₃₉H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 14 h / -10 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / Inert atmosphere

With pyridine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201103270

Reference yield:

: 1335098-47-9
C₃₉H₇₀O₆Si₂

: 1335098-51-5
C₃₉H₆₈O₇Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201103270