C₂₇H₂₇⁽²⁾H₁₈N₅O₅

Base Information

• Chemical Name: C₂₇H₂₇⁽²⁾H₁₈N₅O₅
• CAS No.: 1158083-51-2
• Molecular Formula: C₂₇H₄₅N₅O₅
• Molecular Weight: 537.542

Synonyms:C₂₇H₂₇⁽²⁾H₁₈N₅O₅

Chemical Property of C₂₇H₂₇⁽²⁾H₁₈N₅O₅

Chemical Property:

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Technology Process of C₂₇H₂₇⁽²⁾H₁₈N₅O₅

There total 1 articles about C₂₇H₂₇⁽²⁾H₁₈N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butylaldehyde-d9 (90137-14-7) → C27H27(2)H18N5O5 (1158083-51-2)

Guidance literature:

Multi-step reaction with 11 steps

1.1: acetic acid / water / 22.5 h / 20 - 70 °C

2.1: sulfuric acid / dichloromethane / 0 - 20 °C

2.2: pH 9 / Cooling with ice

3.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 20 °C / 1551.49 Torr

3.2: pH 9

4.1: hydrogenchloride; water / 24 h / Reflux

5.1: triethylamine / 1,4-dioxane; water / 6 h / 20 °C

6.1: 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C

7.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

8.1: triethylamine / 1,4-dioxane

8.2: -78 - 20 °C

9.1: lithium hydroxide / tetrahydrofuran; water / 3 h

10.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C

11.1: dichloro-acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / toluene / 0 - 20 °C

With 4-methyl-morpholine; hydrogenchloride; dichloro-acetic acid; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

DOI:10.1002/jlcr.1905

upstream raw materials:

tert-butylaldehyde-d₉

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