C₅₁H₉₃O₁₁Si₂N

Base Information

Chemical Name:C₅₁H₉₃O₁₁Si₂N
CAS No.:930803-39-7
Molecular Formula:C₅₁H₉₃NO₁₁Si₂
Molecular Weight:952.471
Hs Code.:

C<sub>51</sub>H<sub>93</sub>O<sub>11</sub>Si<sub>2</sub>N

Synonyms:C₅₁H₉₃O₁₁Si₂N

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Chemical Property of C₅₁H₉₃O₁₁Si₂N

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Technology Process of C₅₁H₉₃O₁₁Si₂N

There total 37 articles about C₅₁H₉₃O₁₁Si₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 930803-59-1
C₅₁H₉₇O₁₁Si₂N

: 930803-39-7
C₅₁H₉₃O₁₁Si₂N

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1002/anie.200604053

Reference yield: 99.0%

: 930803-62-6
C₅₁H₉₇O₁₁Si₂N

: 930803-39-7
C₅₁H₉₃O₁₁Si₂N

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-25-1
C₁₀H₁₅S₂O₂Br

: 930803-39-7
C₅₁H₉₃O₁₁Si₂N

Guidance literature:: Multi-step reaction with 10 steps

1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

2: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

3: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

4: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

5: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

6: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

7: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

8: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

9: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 20 °C / pH 7

10: 99 percent / (COCl)2; dimethyl sulfoxide; triethylamine / CH₂Cl₂

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; oxalyl dichloride; tert.-butyl lithium; diisobutylaluminium hydride; lithium triethylborohydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 10: Swern oxidation;
DOI:10.1002/anie.200604053