(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone

Base Information

• Chemical Name: (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone
• CAS No.: 197916-21-5
• Molecular Formula: C₇₁H₉₆O₁₉
• Molecular Weight: 1253.53

Synonyms:(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone

Chemical Property of (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone

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Technology Process of (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone

There total 2 articles about (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid (197916-20-4) → (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3glu-lactone (197916-21-5)

Guidance literature:

With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In benzene; for 16h;

DOI:10.1021/jo971413u

Reference yield: 24.0%

(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid (197916-20-4) → (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3glu-lactone (197916-21-5) + (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 2rha-lactone

Guidance literature:

With dmap; 4-N,N-dimethylaminopyridine trifluoroacetate; dicyclohexyl-carbodiimide; In chloroform; for 21h; Heating;

DOI:10.1021/jo971413u

Reference yield:

(S)-2-Methylbutyric acid (1730-91-2) + (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3glu-lactone (197916-21-5) → (11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-[2,4-di-O-[(2S)-2-methylbutyryl]-α-L-rhamnopyranosyl]-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3glu-lactone (197853-54-6)

Guidance literature:

With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In benzene; for 2.5h;

DOI:10.1021/jo971413u

upstream raw materials:

(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-(α-L-rhamnopyranosyl)-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid

Downstream raw materials:

(11S)-11-[[(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-[2,4-di-O-[(2S)-2-methylbutyryl]-α-L-rhamnopyranosyl]-(1->2)-(4,6-O-benzylidene-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoic acid 3_glu-lactone

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