2,3,5-tribromonitrobenzene

Base Information

• Chemical Name: 2,3,5-tribromonitrobenzene
• CAS No.: 116529-58-9
• Molecular Formula: C₆H₂Br₃NO₂
• Molecular Weight: 359.799
• Mol file: 116529-58-9.mol

Synonyms:2,3,5-tribromonitrobenzene

Chemical Property of 2,3,5-tribromonitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5-tribromonitrobenzene

There total 1 articles about 2,3,5-tribromonitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4-dibromo-6-nitroaniline (827-23-6) → 2,3,5-tribromonitrobenzene (116529-58-9)

Guidance literature:

With tert.-butylnitrite; copper(ll) bromide; In acetonitrile; at 60 ℃; for 1h;

DOI:10.1016/j.tetlet.2009.09.083

Reference yield: 40.0%

2,3,5-tribromonitrobenzene (116529-58-9) + 3,5-dibromo-2-methoxyphenol potassium salt (102740-07-8) → 4,6-dibromo-2-(4',6'-dibromo-2'-nitrophenoxy)anisole (169901-66-0)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃; for 3h;

DOI:10.1007/BF00630523

Reference yield:

2,3,5-tribromonitrobenzene (116529-58-9) → 1,3,5-trisbromobenzene (626-39-1)

Guidance literature:

Multi-step reaction with 4 steps

1: alcohol; ammonia / 140 °C

3: tin; hydrochloric acid

4: durch Ueberfuehrung in das Diazoniumperbromid und dessen Zersetzung mit Alkohol

With hydrogenchloride; tin; ethanol; ammonia;

upstream raw materials:

2,4-dibromo-6-nitroaniline

Downstream raw materials:

2,4-dibromo-6-nitroaniline

2,3,5-tribromo-aniline

4,6-dibromo-2-(4',6'-dibromo-2'-nitrophenoxy)anisole

4,6-dibromo-2-(4',6'-dibromo-2'-hydroxyphenoxy)anisole