N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Base Information

Chemical Name:N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine
CAS No.:835627-05-9
Molecular Formula:C₁₉H₁₇F₆NO₂
Molecular Weight:405.34
Hs Code.:

<i>N</i>-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Synonyms:N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Chemical Property:

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Technology Process of N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

There total 8 articles about N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1027286-16-3
C₂₉H₃₃F₆NO₆

: 835627-05-9
N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2004.04.058

Reference yield:

: 741683-48-7
1-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-ethanone

: 835627-05-9
N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / 12 h / 0 - 25 °C

2: DIBAL / tetrahydrofuran / 2 h / 0 - 25 °C

3: Ph₃P; DEAD / tetrahydrofuran / 20 °C

4: 82 percent / TFA / CH₂Cl₂ / 20 °C

With sodium hydride; diisobutylaluminium hydride; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.04.058

Reference yield:

: (E)-3-[3-(3,5-Bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-en-1-ol

: 835627-05-9
N-{3-[3-(3,5-bis-trifluoromethyl-phenoxymethyl)-phenyl]-but-2-enyl}-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: Ph₃P; DEAD / tetrahydrofuran / 20 °C

2: 82 percent / TFA / CH₂Cl₂ / 20 °C

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.04.058