7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Base Information

Chemical Name:7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane
CAS No.:852359-99-0
Molecular Formula:C₄₀H₆₄Cl₂N₂O₈
Molecular Weight:771.863
Hs Code.:

Synonyms:7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

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Chemical Property of 7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

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Technology Process of 7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

There total 2 articles about 7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 79520-80-2
1,4-bis(4-chlorobutoxy)benzene

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 852359-99-0
7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Guidance literature:: With sodium carbonate; potassium iodide; In various solvent(s); for 72h; Heating;
DOI:10.1016/j.bmc.2005.01.064

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 852359-99-0
7,16-bis-{4-[4-(4-chloro-butoxy)-phenoxy]-butyl}-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / various solvent(s) / 48 h / Heating

2: 41 percent / Na₂CO₃; KI / various solvent(s) / 72 h / Heating

With sodium carbonate; potassium carbonate; potassium iodide; In various solvent(s);
DOI:10.1016/j.bmc.2005.01.064