Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

Base Information

Chemical Name:Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime
CAS No.:121750-91-2
Molecular Formula:C₁₄H₁₇N₃O₃
Molecular Weight:275.307
Hs Code.:

Synonyms:Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

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Chemical Property of Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

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Technology Process of Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

There total 3 articles about Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 103-71-9
phenyl isocyanate

: 121750-98-9
1-hydroxy-1,2,5,6-tetrahydropyridine-3-carboxaldehyde-O-methyloxime

: 121750-91-2,145071-60-9
Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

Guidance literature:: In toluene; at 20 ℃;
DOI:10.1016/0223-5234(92)90186-5

Reference yield:

: 72989-57-2
pyridine-3-carboxaldehyde-O-methyloxime-N-oxide

: 121750-91-2,145071-60-9
Methyl ether of 1-phenylaminocarbonyloxy 1,2,5,6-tetrahydropyridin-3-carboxaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 1 h / Ambient temperature

2: 80 percent / toluene / 20 °C

With sodium tetrahydroborate; In methanol; toluene;
DOI:10.1016/0223-5234(92)90186-5