Technology Process of C15H17N5O4
There total 7 articles about C15H17N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; zinc dibromide;
In
water; isopropyl alcohol;
for 4h;
Reflux;
DOI:10.1021/jo300412j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / ethanol; water / 20 °C
2: thionyl chloride / 4 h / 20 °C
3: thionyl chloride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
4: sodium azide; zinc dibromide / water; isopropyl alcohol / 4 h / Reflux
With
thionyl chloride; sodium azide; sodium hydrogencarbonate; zinc dibromide;
In
ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo300412j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
2: sodium azide; zinc dibromide / water; isopropyl alcohol / 4 h / Reflux
With
thionyl chloride; sodium azide; zinc dibromide;
In
water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo300412j