C₁₆H₁₇ClN₂O

Base Information

Chemical Name:C₁₆H₁₇ClN₂O
CAS No.:1332336-72-7
Molecular Formula:C₁₆H₁₇ClN₂O
Molecular Weight:288.777
Hs Code.:

C<sub>16</sub>H<sub>17</sub>ClN<sub>2</sub>O

Synonyms:C₁₆H₁₇ClN₂O

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Chemical Property of C₁₆H₁₇ClN₂O

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Technology Process of C₁₆H₁₇ClN₂O

There total 6 articles about C₁₆H₁₇ClN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1332336-71-6
C₁₆H₁₅ClN₂O

: 1332336-72-7
C₁₆H₁₇ClN₂O

Guidance literature:: With sodium tetrahydroborate; In ethanol; water;
DOI:10.1016/j.bmcl.2011.06.014

Reference yield:

: 884495-38-9
6-chloro-4-methylnicotinaldehyde

: 1332336-72-7
C₁₆H₁₇ClN₂O

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene

2: toluene-4-sulfonic acid / tetrahydrofuran

3: sodium hydride / N,N-dimethyl-formamide

4: ammonia / methanol / Reflux

5: sodium tetrahydroborate / ethanol; water

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; sodium hydride; sodium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.06.014

Reference yield:

: 1332336-58-9
C₁₃H₁₀ClNO

: 1332336-72-7
C₁₆H₁₇ClN₂O

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / tetrahydrofuran

2: sodium hydride / N,N-dimethyl-formamide

3: ammonia / methanol / Reflux

4: sodium tetrahydroborate / ethanol; water

With sodium tetrahydroborate; ammonia; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.06.014