5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid

Base Information

• Chemical Name: 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid
• CAS No.: 1542497-26-6
• Molecular Formula: C₂₇H₂₇N₃O₇
• Molecular Weight: 505.527

Synonyms:5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid

Chemical Property of 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid

Chemical Property:

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Technology Process of 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid

There total 2 articles about 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

5-Aminosalicylic Acid (89-57-6) + benzyl ((S)-1-(((S)-1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate (820239-47-2) → 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid (1542497-26-6)

Guidance literature:

In water; at 70 ℃; for 2h; Microwave irradiation; Green chemistry;

DOI:10.1055/s-0033-1338532

Reference yield:

N-benzyloxycarbonyl-L-alanyl-L-phenylalanine (2768-53-8) → 5-{(S)-2-[(S)-2-{[(benzyloxy)carbonyl]amino}propanamido]-3-phenylpropanamido}-2-hydroxybenzoic acid (1542497-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: water / 2 h / 70 °C / Microwave irradiation; Green chemistry

With thionyl chloride; In water;

DOI:10.1055/s-0033-1338532

upstream raw materials:

N-benzyloxycarbonyl-L-alanyl-L-phenylalanine

5-Aminosalicylic Acid

benzyl ((S)-1-(((S)-1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

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