Technology Process of C24H22N2O3
There total 5 articles about C24H22N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine; acetic acid;
In
methanol;
at 40 ℃;
Reflux;
DOI:10.1002/cmdc.201200296
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonium cerium (IV) nitrate / acetonitrile / 0.25 h / -35 - 20 °C
2: ammonium acetate; acetic acid / 48 h / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C
4: N,N-dimethyl-formamide / 190 °C / Microwave irradiation
5: hydroxylamine; acetic acid / methanol / 40 °C / Reflux
With
ammonium cerium (IV) nitrate; ammonium acetate; hydroxylamine; sodium hydride; acetic acid;
In
methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200296
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 190 °C / Microwave irradiation
2: hydroxylamine; acetic acid / methanol / 40 °C / Reflux
With
hydroxylamine; acetic acid;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200296