Technology Process of C11H11ClF3NO5S2
There total 11 articles about C11H11ClF3NO5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
Reflux;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: borane-THF / tetrahydrofuran / 0 - 20 °C
2: pyridine / dichloromethane / 0 - 20 °C
3: N,N-dimethyl-formamide / 20 - 70 °C
4: hydrogenchloride; iron / water; methanol / 3 h / Reflux
5: triethylamine / dichloromethane / 3 h / 0 - 20 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Reflux
7: chlorosulfonic acid / 0 - 20 °C / Neat (no solvent)
8: thionyl chloride / Reflux
With
pyridine; hydrogenchloride; chlorosulfonic acid; thionyl chloride; borane-THF; iron; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: N,N-dimethyl-formamide / 5 h / 50 °C
2: hydrogenchloride / methanol / 20 °C
3: tetrahydrofuran; methanol / 0 - 20 °C
4: pyridine / dichloromethane / 0 - 20 °C
5: N,N-dimethyl-formamide / 20 - 70 °C
6: hydrogenchloride; iron / water; methanol / 3 h / Reflux
7: triethylamine / dichloromethane / 3 h / 0 - 20 °C
8: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Reflux
9: chlorosulfonic acid / 0 - 20 °C / Neat (no solvent)
10: thionyl chloride / Reflux
With
pyridine; hydrogenchloride; chlorosulfonic acid; thionyl chloride; iron; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;