allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside

Base Information

• Chemical Name: allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside
• CAS No.: 314038-14-7
• Molecular Formula: C₄₈H₅₂O₈Si
• Molecular Weight: 785.022

Synonyms:allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside

Chemical Property of allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside

There total 1 articles about allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl chloride (76-83-5) → allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside (314038-14-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 4-dimethylaminopyridine / pyridine / 16 h / 80 °C

2: dimethylformamide / 20 °C

3: 6.19 g / pyridine / dimethylformamide / 50 °C

With pyridine; dmap; In pyridine; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(00)01161-3

Reference yield: 91.0%

allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside (314038-14-7) → allyl 2,4-di-O-benzoyl-α-D-mannopyranoside (314038-22-7)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 4h;

DOI:10.1016/S0040-4020(00)01161-3

Reference yield: 88.0%

allyl 2,4-di-O-benzoyl-3-O-tert-butyldimethylsilyl-6-O-triphenylmethyl-α-D-mannopyranoside (314038-14-7) → C29H38O8Si

Guidance literature:

With iron(III) chloride; In dichloromethane;

DOI:10.1016/S0040-4020(00)01161-3

upstream raw materials:

trityl chloride

Downstream raw materials:

allyl 2,4-di-O-benzoyl-α-D-mannopyranoside

C₉H₁₃O₆(C₇H₅O)2C₁₉H₁₅

allyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4-di-O-benzoyl-α-D-mannopyranoside

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