N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

Base Information

Chemical Name:N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine
CAS No.:197727-29-0
Molecular Formula:C₃₀H₃₅N₆O₁₂P
Molecular Weight:702.615
Hs Code.:

Synonyms:N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

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Chemical Property of N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

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Technology Process of N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

There total 17 articles about N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 197727-26-7
N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine methyl ester

: 197727-29-0
N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

Guidance literature:: With cysteine buffer; protease papain from Carica papaya; at 37 ℃;
DOI:10.1039/a704215i

Reference yield: 92.0%

: 221351-02-6
N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine-methoxyethoxyethyl ester

: 197727-29-0
N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

Guidance literature:: With phosphate buffer; L-Cysteine; papain; In acetone; at 37 ℃;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<669::AID-CHEM669>3.0.CO;2-V

Reference yield:

: 203986-32-7
3'-O-Acetyl-5'-O-dimethoxytrityl-6-N-phenylacetyl-2'-deoxyadenosine

: 197727-29-0
N-Allyloxycarbonyl-O-(3'-O-acetyl-6-N-phenylacetyl-2'-deoxyadenosyl-allyl-phosphato)-L-serine

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / ZnBr₂ / nitromethane / 0.25 h / Ambient temperature

2: tetrazole / CH₂Cl₂; acetonitrile / 18 h / Ambient temperature

3: tBuOOH / CH₂Cl₂ / 0.17 h / 0 °C

4: 96 percent / papain, L-cysteine, phosphate buffer (pH 6.6) / acetone / 37 °C

With 1H-tetrazole; tert.-butylhydroperoxide; phosphate buffer; L-Cysteine; zinc dibromide; papain; In nitromethane; dichloromethane; acetone; acetonitrile;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<669::AID-CHEM669>3.0.CO;2-V