Technology Process of C34H50N6O9
There total 14 articles about C34H50N6O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 2h;
under 760.051 Torr;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.01.084
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dicyclohexyl-carbodiimide / tetrahydrofuran / 16 h / 20 °C
2: sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / 20 °C
3: hydrogen bromide; acetic acid / dichloromethane / 0.5 h / 20 °C
4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere
5: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.01.084
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / 20 °C
2: hydrogen bromide; acetic acid / dichloromethane / 0.5 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.01.084
