(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

Base Information

Chemical Name:(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester
CAS No.:335317-39-0
Molecular Formula:C₂₂H₂₃NO₆
Molecular Weight:397.428
Hs Code.:

Synonyms:(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

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Chemical Property of (2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

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Technology Process of (2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

There total 7 articles about (2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 335317-38-9
(2R,3S)-3-Allyloxycarbonylamino-2-hydroxy-3-phenyl-propionic acid methyl ester

: 335317-39-0
(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

Guidance literature:: With camphor-10-sulfonic acid; In toluene; for 5h; Heating;
DOI:10.3987/COM-00-S(I)34

Reference yield:

: 99458-15-8
Methyl (2R,3S)-(+)-2-hydroxy-3-azido-3-phenyl-propionate

: 335317-39-0
(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: PPh₃; H₂O / tetrahydrofuran / 12 h / 20 °C

2: NaHCO₃ / diethyl ether / 12 h / 20 °C

3: 93 percent / CSA / toluene / 5 h / Heating

With camphor-10-sulfonic acid; water; sodium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.3987/COM-00-S(I)34

Reference yield:

: 122743-18-4
methyl (2R,3S)-2,3-dihydroxy-3-phenylpropanoate

: 335317-39-0
(2S,4S,5R)-2-(4-Methoxy-phenyl)-4-phenyl-oxazolidine-3,5-dicarboxylic acid 3-allyl ester 5-methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: HBr / 4 h / 20 °C

2: NaN₃ / dimethylformamide / 20 h / 60 °C

3: AcCl; MeOH / 12 h / 20 °C

4: PPh₃; H₂O / tetrahydrofuran / 12 h / 20 °C

5: NaHCO₃ / diethyl ether / 12 h / 20 °C

6: 93 percent / CSA / toluene / 5 h / Heating

With methanol; sodium azide; camphor-10-sulfonic acid; water; hydrogen bromide; sodium hydrogencarbonate; acetyl chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-00-S(I)34