1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether

Base Information

• Chemical Name: 1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether
• CAS No.: 174318-92-4
• Molecular Formula: C₂₉H₃₃NO₅
• Molecular Weight: 475.585
• Mol file: 174318-92-4.mol

Synonyms:1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether

Chemical Property of 1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether

There total 1 articles about 1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(E)-3,4-dibenzyloxy-β-nitrostyrene (1699-54-3) + cyclohexanemethanol sodium salt (108122-41-4) → 1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether (174318-92-4)

Guidance literature:

In various solvent(s); Ambient temperature;

DOI:10.1016/0223-5234(96)88314-0

Reference yield: 32.0%

1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether (174318-92-4) → 2-cyclohexylmethyloxy-2-(3,4-dibenzyloxyphenyl)ethylamine (174318-98-0)

Guidance literature:

With hydrogen; platinum on activated charcoal; In ethanol; for 20h; under 760 Torr;

DOI:10.1016/0223-5234(96)88314-0

Reference yield:

1-(3,4-dibenzyloxyphenyl)-2-nitroethylmethylcyclohexyl ether (174318-92-4) → 2-cyclohexylmethyloxy-2-(3,4-dihydroxyphenyl)ethylamine

Guidance literature:

Multi-step reaction with 2 steps

1: 32 percent / H₂ / 10percent Pt/C / ethanol / 20 h / 760 Torr

2: 97 percent / H₂ / 5percent Pd/C / ethanol / 2.5 h / 760 Torr

With hydrogen; palladium on activated charcoal; platinum on activated charcoal; In ethanol;

DOI:10.1016/0223-5234(96)88314-0

upstream raw materials:

(E)-3,4-dibenzyloxy-β-nitrostyrene

cyclohexanemethanol sodium salt

Downstream raw materials:

2-cyclohexylmethyloxy-2-(3,4-dibenzyloxyphenyl)ethylamine

Refernces