4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside
CAS No.:1603837-20-2
Molecular Formula:C₂₉H₂₉NO₉
Molecular Weight:535.551
Hs Code.:

Synonyms:4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

There total 6 articles about 4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1603837-19-9
4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-6-O-[(tert-butyl)(diphenyl)silyl]-2-deoxy-β-D-glucopyranoside

: 1603837-20-2
4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/hlca.201300195

Reference yield:

: 38229-72-0
4-methoxyphenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 1603837-20-2
4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methylate / methanol / 0.5 h / 20 °C

2: pyridine / 6 h / 20 °C

3: 5 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.201300195

Reference yield:

: C₃₁H₃₉NO₇Si

: 1603837-20-2
4-methoxyphenyl 2-(acetylamino)-3,4-di-O-benzoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 5 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1002/hlca.201300195