3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide

Base Information

• Chemical Name: 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide
• CAS No.: 382617-08-5
• Molecular Formula: C₂₁H₂₁N₃O₃
• Molecular Weight: 363.416

Synonyms:3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide

Chemical Property of 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide

Chemical Property:

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Technology Process of 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide

There total 6 articles about 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1]naphthyl-(3-nitro-phenyl)-diazene (77812-69-2) → 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide (382617-08-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaSH / ethanol; H₂O

2: dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide

With sodium hydrogensulfide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(01)01347-8

Reference yield:

3-nitrophenyldiazonium chloride (2028-76-4) → 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide (382617-08-5)

Guidance literature:

Multi-step reaction with 5 steps

1: HCl / H₂O

2: H₂SO₄; NaNO₂ / acetic acid

3: H₃PO₂ / H₂O

4: NaSH / ethanol; H₂O

5: dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide

With hydrogenchloride; sodium hydrogensulfide; sulfuric acid; hypophosphorous acid; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In ethanol; water; acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(01)01347-8

Reference yield:

1-amino-naphthalene (134-32-7) → 3-hydroxy-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide (382617-08-5)

Guidance literature:

Multi-step reaction with 5 steps

1: HCl / H₂O

2: H₂SO₄; NaNO₂ / acetic acid

3: H₃PO₂ / H₂O

4: NaSH / ethanol; H₂O

5: dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide

With hydrogenchloride; sodium hydrogensulfide; sulfuric acid; hypophosphorous acid; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In ethanol; water; acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(01)01347-8

upstream raw materials:

2,2-bis(hydroxymethyl)propionic acid

3-(naphthalen-1-ylazo)-phenylamine

[1]naphthyl-(3-nitro-phenyl)-diazene

3-nitrophenyldiazonium chloride

Downstream raw materials:

3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-hydroxymethyl-2-methyl-N-[3-(naphthalen-1-ylazo)-phenyl]-propionamide

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