(E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde

Base Information

• Chemical Name: (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde
• CAS No.: 1385014-55-0
• Molecular Formula: C₃₇H₄₂OS₃
• Molecular Weight: 598.938

Synonyms:(E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde

Chemical Property of (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde

There total 1 articles about (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(1,3-dioxolan-2-yl)thiophene-2-carboxaldehyde (52509-15-6) + diethyl (E,E)-3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]benzylphosphonate (1385014-54-9) → (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde (1385014-55-0)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo301054w

Reference yield: 83.0%

(E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde (1385014-55-0) + 1,3,5-tris(diethoxyphosphorylmethyl)benzene (6566-57-0) → C120H132S9 (1385014-62-9)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -40 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo301054w

Reference yield:

methyl 3,5-bis[(diethoxyphosphoryl)methyl]benzoate (1202493-19-3) + (E,E,E)-5-{3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]styryl}thiophene-2-carboxaldehyde (1385014-55-0) → C84H92O2S6

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -40 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo301054w

upstream raw materials:

5-(1,3-dioxolan-2-yl)thiophene-2-carboxaldehyde

diethyl (E,E)-3,5-bis[2-(5-hexylthiophen-2-yl)vinyl]benzylphosphonate

Downstream raw materials:

C₁₂₀H₁₃₂S₉

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