2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

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Chemical Name:2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone
CAS No.:915769-92-5
Molecular Formula:C₅₃H₅₂O₁₀
Molecular Weight:848.99
Hs Code.:

Synonyms:2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

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Chemical Property of 2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

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Technology Process of 2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

There total 1 articles about 2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 915778-71-1
C₆₁H₇₀O₁₀Si₂

: 915769-92-5
2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

Guidance literature:: C₆₁H₇₀O₁₀Si₂; With potassium hydroxide; water; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

With hydrogenchloride; In ethanol; at 65 ℃; for 4h;
DOI:10.1021/ja0652619

Reference yield: 74.0%

: 915769-92-5
2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

: 915769-93-6
2-(2-benzyloxy-4-hydroxy-2-methyl-butyl)-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at -15 ℃;
DOI:10.1021/ja0652619

Reference yield:

: 915769-92-5
2-[2-benzyloxy-4-(4-methoxy-phenoxy)-2-methyl-butyl]-6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-anthraquinone

: 3-benzyloxy-4-[6-(4,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yl)-1,5-dihydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yl]-3-methyl-butyraldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.33 h / -15 °C

2: IBX / ethyl acetate / 3 h / 80 °C

With ammonium cerium(IV) nitrate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tet.2007.04.031