trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

Base Information

Chemical Name:trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))
CAS No.:18665-82-2
Molecular Formula:C₁₅H₂₆O
Molecular Weight:222.371
Hs Code.:

Synonyms:trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

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Chemical Property of trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

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Technology Process of trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

There total 5 articles about trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 42569-34-6
ethyl (Z)-3-methyl-5-(2',6',6'-trimethylcyclohex-1'-en-1'-yl)pent-2-enoate

: 18665-82-2
trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 0 ℃;
DOI:10.1016/S0040-4039(00)00639-0

Reference yield:

: 17283-81-7
4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on

: 18665-82-2
trans-Monocyclo-farnesol,(trans-3-Methyl-5-<2,6,6-trimethyl-cyclohexenyl-(1)>-penten-(2)-ol-(1))

Guidance literature:: Multi-step reaction with 2 steps

1: 9 percent / LiHMDS / tetrahydrofuran / 5 h / Heating

2: 100 percent / DIBALH / toluene / 0 °C

With diisobutylaluminium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 1: Horner-Emmons olefination;
DOI:10.1246/bcsj.78.1197