C₂₅H₁₉N₃

Base Information

Chemical Name:C₂₅H₁₉N₃
CAS No.:1450729-47-1
Molecular Formula:C₂₅H₁₉N₃
Molecular Weight:361.446
Hs Code.:

C<sub>25</sub>H<sub>19</sub>N<sub>3</sub>

Synonyms:C₂₅H₁₉N₃

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Chemical Property of C₂₅H₁₉N₃

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Technology Process of C₂₅H₁₉N₃

There total 5 articles about C₂₅H₁₉N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 106-38-7
para-bromotoluene

: 1450729-39-1
C₁₉H₁₅N₃S

: 1450729-47-1
C₂₅H₁₉N₃

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); magnesium; ethylene dibromide; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1055/s-0033-1338951

Reference yield:

: 1450729-32-4
7-(tert-butoxycarbonyl)-4-chloro-2-methylthio-7H-pyrrolo[2,3-d]pyrimidine

: 1450729-47-1
C₂₅H₁₉N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: CyJohnPhos; palladium diacetate / 1,4-dioxane / 0.17 h / Inert atmosphere

1.2: 1 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

3.1: potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 13 h / Inert atmosphere; Reflux

4.1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); magnesium; ethylene dibromide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); trans-1,2-Diaminocyclohexane; palladium diacetate; magnesium; ethylene dibromide; trifluoroacetic acid; CyJohnPhos; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 1.1: |Suzuki Coupling / 1.2: |Suzuki Coupling / 4.1: |Kumada Cross-Coupling;
DOI:10.1055/s-0033-1338951

Reference yield:

: 1450729-33-5
C₁₈H₁₉N₃O₂S

: 1450729-47-1
C₂₅H₁₉N₃

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

2: potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 13 h / Inert atmosphere; Reflux

3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); magnesium; ethylene dibromide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); trans-1,2-Diaminocyclohexane; magnesium; ethylene dibromide; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 3: |Kumada Cross-Coupling;
DOI:10.1055/s-0033-1338951