3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

Base Information

Chemical Name:3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one
CAS No.:1623093-69-5
Molecular Formula:C₂₃H₂₀N₂O₆
Molecular Weight:420.422
Hs Code.:

Synonyms:3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

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Chemical Property of 3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

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Technology Process of 3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

There total 5 articles about 3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 3-acetyl-(E)-N-(4-methylbenzylidene)coumarin-4-oxyacetic hydrazine

: 108-24-7
acetic anhydride

: 1623093-69-5
3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

Guidance literature:: for 8h; Reflux;
DOI:10.3390/molecules19010911

Reference yield:

: 15059-36-6
4-acetoxycoumarin

: 1623093-69-5
3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 4 h / 180 °C

2: potassium carbonate / acetone / 10 h / Reflux

3: hydrazine hydrate / methanol / 7 h / 20 °C

4: acetic acid / methanol; water / 5 h / Reflux

5: 8 h / Reflux

With hydrazine hydrate; potassium carbonate; acetic acid; In methanol; water; acetone;
DOI:10.3390/molecules19010911

Reference yield:

: 1076-38-6,92395-12-5
4-hydroxy[1]benzopyran-2-one

: 1623093-69-5
3-acetyl-4-((4-acetyl-5-(4-methylphenyl)-4,5-dihydro-1,3,4-oxodiazol-2-yl)methoxy)-2H-chromen-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: 2 h / 150 °C

2: 4 h / 180 °C

3: potassium carbonate / acetone / 10 h / Reflux

4: hydrazine hydrate / methanol / 7 h / 20 °C

5: acetic acid / methanol; water / 5 h / Reflux

6: 8 h / Reflux

With hydrazine hydrate; potassium carbonate; acetic acid; In methanol; water; acetone;
DOI:10.3390/molecules19010911