7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

Base Information

Chemical Name:7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine
CAS No.:146722-72-7
Molecular Formula:C₂₄H₂₇N₃O₂
Molecular Weight:389.497
Hs Code.:

Synonyms:7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

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Chemical Property of 7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

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Technology Process of 7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

There total 2 articles about 7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 146722-70-5
2-Chloro-7,8-dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

: 146722-72-7
7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

Guidance literature:: With hydrogen; sodium acetate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; for 1h; under 1292.9 Torr;
DOI:10.1016/S0040-4020(01)80524-X

Reference yield:

: 146722-75-0
7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidin-2(1H)-one

: 146722-72-7
7,8-Dimethoxy-3,5-dimethyl-4-mesitylimino-3,4-dihydro-5H-indeno<1,2-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / POCl₃, 4-dimethylaminopyridine / 3.5 h / Heating

2: 65 percent / H₂, CH₃COONa / 5percent Pd/C / dimethylformamide; methanol / 1 h / 1292.9 Torr

With dmap; hydrogen; sodium acetate; trichlorophosphate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80524-X