6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

Base Information

Chemical Name:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil
CAS No.:79872-70-1
Molecular Formula:C₁₆H₂₁N₅O₄
Molecular Weight:347.374
Hs Code.:

Synonyms:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

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Chemical Property of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

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Technology Process of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

There total 6 articles about 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18636-32-3
3-methyllumiflavin

: 79872-70-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) dithionite, NaOH / 1.) aq. ethanol, ice bath, 1 h, 2.) room temperature; 50-55 deg C, 5 h

2: 30.2 percent / sodium hydrogen carbonate, m-chloroperbenzoic acid / CHCl₃ / 0.5 h

3: 70.5 percent / dithionite,aq. sodium chloride / CHCl₃ / 0.03 h / acetate buffer

4: 24 h

5: 1.) N,N-dimethylaniline, 2.) acetic acid / 1.) methanol

With sodium hydroxide; sodium dithionite; sodium hydrogencarbonate; dithionite^(2-); acetic acid; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In chloroform;
DOI:10.1021/ja00352a045

Reference yield:

: 40815-89-2
3,5,5-trimethyl-1,5-dihydrolumiflavin

: 79872-70-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

Guidance literature:: Multi-step reaction with 4 steps

1: 30.2 percent / sodium hydrogen carbonate, m-chloroperbenzoic acid / CHCl₃ / 0.5 h

2: 70.5 percent / dithionite,aq. sodium chloride / CHCl₃ / 0.03 h / acetate buffer

3: 24 h

4: 1.) N,N-dimethylaniline, 2.) acetic acid / 1.) methanol

With sodium hydrogencarbonate; dithionite^(2-); acetic acid; N,N-dimethyl-aniline; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In chloroform;
DOI:10.1021/ja00352a045

Reference yield:

: 79854-08-3
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione

: 79872-70-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

Guidance literature:: Multi-step reaction with 3 steps

1: 70.5 percent / dithionite,aq. sodium chloride / CHCl₃ / 0.03 h / acetate buffer

2: 24 h

3: 1.) N,N-dimethylaniline, 2.) acetic acid / 1.) methanol

With dithionite^(2-); acetic acid; N,N-dimethyl-aniline; sodium chloride; In chloroform;
DOI:10.1021/ja00352a045