N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester
CAS No.:122148-92-9
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

Synonyms:N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

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Chemical Property of N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

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Technology Process of N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

There total 7 articles about N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79722-21-7
tert-butyl N-(benzyloxy)carbamate

: 106-95-6
allyl bromide

: 122148-92-9
N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 1h;
DOI:10.1016/S0040-4039(01)80314-2

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 122148-92-9
N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / 1,4-dioxane

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C

2.2: 1 h / 20 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2ob25073j

Reference yield:

: 29601-98-7
N-benzylhydroxylamine hydrochloride

: 122148-92-9
N-(phenylmethoxy)-N-2-propenylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaHCO₃ / H₂O; dioxane / 2 h / Ambient temperature

2: 99 percent / NaH / dimethylformamide / 1 h / 50 °C

With sodium hydride; sodium hydrogencarbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)80314-2