dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

Base Information

Chemical Name:dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate
CAS No.:1009089-90-0
Molecular Formula:C₂₉H₄₇O₆PSi₂
Molecular Weight:578.833
Hs Code.:

Synonyms:dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

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Chemical Property of dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

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Technology Process of dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

There total 1 articles about dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 667421-82-1
methyl (3S)-4-tert-butyldiphenylsiloxy-3-triethylsiloxybutanoate

: 756-79-6
dimethyl methane phosphonate

: 1009089-90-0
dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

methyl (3S)-4-tert-butyldiphenylsiloxy-3-triethylsiloxybutanoate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo7023152

Reference yield: 98.0%

: 910228-57-8
C₁₆H₂₂O₄

: 1009089-90-0
dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate

: 1009089-94-4
(2S,5E,7S)-1-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-7-[(4S,5S)-5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]-2-[(1,1,1-triethylsilyl)oxy]-5-octen-4-one

Guidance literature:: dimethyl (4S)-5-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-oxo-4-[(triethylsilyl)oxy]pentylphosphonate; With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 0.5h;

C₁₆H₂₂O₄; In acetonitrile; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/jo7023152