Zirconylperchlorate

Base Information

• Chemical Name: Zirconylperchlorate
• CAS No.: 15607-09-7
• Molecular Formula: 2ClO₄*OZr
• Molecular Weight: 306.125
• Mol file: 15607-09-7.mol

Synonyms:Zirconium,oxobis(perchlorato-O)-; Zirconium, oxodiperchlorato-, ZrO(ClO4)2 (8CI);Zirconyl perchlorate (7CI); Perchloric acid, zirconium complex; Zirconyldiperchlorate (ZrO(ClO4)2)

Chemical Property of Zirconylperchlorate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

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MSDS Files:

Useful:

Technology Process of Zirconylperchlorate

There total 1 articles about Zirconylperchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perchloric acid (7601-90-3) → zirconiumoxide perchlorate (12591-05-8,15607-09-7)

Guidance literature:

With Zirkonoxydhydrogel (germ.); In water; 25% HClO4 is used;; evapn. and cooling;;

Reference yield:

zirconiumoxide perchlorate (12591-05-8,15607-09-7) + Dibenzyl sulfoxide (621-08-9) → ZrO(2+)*2ClO4(1-)*6(C6H5CH2)2SO=ZrO(ClO4)2*6(C6H5CH2)2SO

Guidance literature:

In ethanol; ZrO(ClO4)2 was dissolved in abs. EtOH and 2,2'-dimethoxy propane, mixt.was warmed on a water bath with stirring, ligand was added, mixt. was refluxed for 2-3 h; excess of solvent was distilled off, ppt. was treated with petroleum ether, ppt. was washed and dried in vac.; elem. anal.;

DOI:10.1016/0040-6031(85)85461-7

Reference yield:

zirconiumoxide perchlorate (12591-05-8,15607-09-7) + 4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one (83-07-8) → ZrO(4-aminoantipyrine)3(ClO4)2

Guidance literature:

In methanol; methanolic soln. of Zr-salt was mixed with methanolic soln. of ligand in the required molar ratio, stirred for 2 h; washed with appropriate solvent and finally with ether and dried in a vac. desiccator over P4O10, elem. anal.;

upstream raw materials:

perchloric acid

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