18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

Base Information

Chemical Name:18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol
CAS No.:812653-08-0
Molecular Formula:C₃₄H₅₁NO₅S
Molecular Weight:585.849
Hs Code.:

18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1<i>H</i>-indol-3-yl]-octadecan-1-ol

Synonyms:18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

Suppliers and Price of 18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

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Technology Process of 18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

There total 15 articles about 18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3-(18-benzyloxy-octadec-1-enyl)-6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indole

: 812653-08-0
18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; under 760 Torr;
DOI:10.1021/jm0493616

Reference yield:

: 3189-13-7
6-methoxylindole

: 812653-08-0
18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / phosphoryl chloride / 0 - 40 °C

2.1: NaOH / CH₂Cl₂ / 20 °C

2.2: 97 percent / CH₂Cl₂ / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0 °C

3.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C

3.3: 66 percent / tetrahydrofuran; hexane / -78 - 0 °C

4.1: 85 percent / H₂ / Pd/C / ethanol / 20 °C / 760 Torr

With sodium hydroxide; n-butyllithium; hydrogen; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; 1.1: Vilsmeier formylation / 3.3: Wittig reaction;
DOI:10.1021/jm0493616

Reference yield:

: 70555-46-3
6-methoxy-1H-indole-3-carbaldehyde

: 812653-08-0
18-[6-methoxy-1-(4-methoxy-benzenesulfonyl)-1H-indol-3-yl]-octadecan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaOH / CH₂Cl₂ / 20 °C

1.2: 97 percent / CH₂Cl₂ / 20 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 0 °C

2.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C

2.3: 66 percent / tetrahydrofuran; hexane / -78 - 0 °C

3.1: 85 percent / H₂ / Pd/C / ethanol / 20 °C / 760 Torr

With sodium hydroxide; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; 2.3: Wittig reaction;
DOI:10.1021/jm0493616