N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine

Base Information

Chemical Name:N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine
CAS No.:15548-02-4
Molecular Formula:C15H21 N O2
Molecular Weight:247.33274
Hs Code.:2928000090
DSSTox Substance ID:DTXSID00369487
Mol file:15548-02-4.mol

Synonyms:15548-02-4;N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine;2-ethyl-2-(3-methoxyphenyl)cyclohexanone oxime;Maybridge3_005188;Oprea1_661828;DTXSID00369487

Suppliers and Price of N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-ETHYL-2-(3-METHOXYPHENYL)CYCLOHEXANONE OXIME 95.00%
5MG
$ 501.28

Total 3 raw suppliers

Chemical Property of N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine

Chemical Property:

Melting Point:97-100 °C(Solv: ligroine (8032-32-4))
Boiling Point:396.1±42.0 °C(Predicted)
PKA:12.26±0.40(Predicted)
PSA：41.82000
Density:1.07±0.1 g/cm3(Predicted)
LogP:3.74720
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:247.157228913
Heavy Atom Count:18
Complexity:303

Purity/Quality:

99% ^*data from raw suppliers

2-ETHYL-2-(3-METHOXYPHENYL)CYCLOHEXANONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(CCCCC1=NO)C2=CC(=CC=C2)OC

Technology Process of N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine

There total 2 articles about N-[2-ethyl-2-(3-methoxyphenyl)cyclohexylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76778-38-6
2-ethyl-2-(3-methoxyphenyl)cyclohexanone

: 15548-02-4
2-ethyl-2-(3-methoxyphenyl)cyclohexanone oxime

Guidance literature:: With sodium hydroxide; hydroxylamine hydrochloride; In methanol; water; at 40 ℃; for 2h;

Reference yield:

: 15547-89-4
2-(3-methoxyphenyl)cyclohexanone

: 15548-02-4
2-ethyl-2-(3-methoxyphenyl)cyclohexanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodamide / 1.) THF, reflux, 90 min, 2.) amb. temp., 16 h

2: 160 g / hydroxylamine hydrochloride, sodium hydroxide / methanol; H₂O / 2 h / 40 °C

With sodium hydroxide; hydroxylamine hydrochloride; sodium amide; In methanol; water;