1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Base Information

Chemical Name:1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide
CAS No.:1446712-56-6
Molecular Formula:C₁₄H₁₄FN₇
Molecular Weight:299.31
Hs Code.:

Synonyms:1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

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Chemical Property of 1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Chemical Property:

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Technology Process of 1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

There total 6 articles about 1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426309-42-3
1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidamide

: 1446712-56-6
1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: With hydrazine hydrate; triethylamine; In ethanol; at 0 - 20 ℃; for 18h;

Reference yield:

: 1276056-73-5
6-methyl-1H-pyrazolo[3,4-d]pyrimidine

: 1446712-56-6
1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide / N,N-dimethyl-formamide / 2 h / 80 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: dimethyl sulfoxide / 2 h / 150 °C

4.1: sodium methylate / methanol / 1.25 h / 20 °C / Inert atmosphere

4.2: 0.75 h / 45 °C / Inert atmosphere

5.1: triethylamine; hydrazine hydrate / ethanol / 18 h / 0 - 20 °C

With N-iodo-succinimide; sodium methylate; caesium carbonate; hydrazine hydrate; triethylamine; In methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1415559-47-5
3-iodo-6-methyl-1H-pyrazolo[3,4-d]pyrimidine

: 1446712-56-6
1-(2-fluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: dimethyl sulfoxide / 2 h / 150 °C

3.1: sodium methylate / methanol / 1.25 h / 20 °C / Inert atmosphere

3.2: 0.75 h / 45 °C / Inert atmosphere

4.1: triethylamine; hydrazine hydrate / ethanol / 18 h / 0 - 20 °C

With sodium methylate; caesium carbonate; hydrazine hydrate; triethylamine; In methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;