(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

Base Information

Chemical Name:(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane
CAS No.:1229041-71-7
Molecular Formula:C₄₀H₆₀O₂SiSn
Molecular Weight:719.711
Hs Code.:

Synonyms:(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

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Chemical Property of (E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

Chemical Property:

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Technology Process of (E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

There total 4 articles about (E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 688-73-3
tri-n-butyl-tin hydride

: 1229041-71-7
(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: copper(I) bromide dimethylsulfide complex; lithium diisopropyl amide / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane / Inert atmosphere

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; dichloromethane / Inert atmosphere

With copper(I) bromide dimethylsulfide complex; di-isopropyl azodicarboxylate; diisobutylaluminium hydride; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 3: |Mitsunobu Displacement;
DOI:10.1021/jo300872y

Reference yield:

: 1229041-69-3
C₃₅H₅₆O₃SiSn

: 1229041-71-7
(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; dichloromethane / Inert atmosphere

With di-isopropyl azodicarboxylate; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2: |Mitsunobu Displacement;
DOI:10.1021/jo300872y

Reference yield:

: 158478-17-2
Methyl 6-(tert-butyldiphenylsiloxy)-2-hexynoate

: 1229041-71-7
(E)-tert-butyl(6-phenoxy-4-(tributylstannyl)hex-4-enyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: copper(I) bromide dimethylsulfide complex; lithium diisopropyl amide / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane / Inert atmosphere

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; dichloromethane / Inert atmosphere

With copper(I) bromide dimethylsulfide complex; di-isopropyl azodicarboxylate; diisobutylaluminium hydride; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 3: |Mitsunobu Displacement;
DOI:10.1021/jo300872y