α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester

Base Information

• Chemical Name: α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester
• CAS No.: 147492-93-1
• Molecular Formula: C₂₈H₄₆N₄O₇
• Molecular Weight: 550.696

Synonyms:α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester

Chemical Property of α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester

Chemical Property:

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Technology Process of α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester

There total 1 articles about α-N-(tert-butoxycarbonyl)-N^G-(benzyloxy)-N^G-methyl-N^G'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-methyl-O-benzylhydroxylamine (22513-22-0) + α-N-(tert-butoxycarbonyl)-δ-<(N1-(tert-butoxycarbonyl)-S-methyl)-1-isothioureido>-L-norvaline tert-butyl ester (133565-51-2) → α-N-(tert-butoxycarbonyl)-NG-(benzyloxy)-NG-methyl-NG'-(tert-butoxycarbonyl)-L-arginine tert-butyl ester (147492-93-1)

Guidance literature:

With silver nitrate; triethylamine; In acetonitrile; at 0 ℃; for 2h;

DOI:10.1021/jm00056a009

upstream raw materials:

N-methyl-O-benzylhydroxylamine

α-N-(tert-butoxycarbonyl)-δ-<(N¹-(tert-butoxycarbonyl)-S-methyl)-1-isothioureido>-L-norvaline tert-butyl ester

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