mesityl 4-bromophenyl ether

Base Information

• Chemical Name: mesityl 4-bromophenyl ether
• CAS No.: 118095-18-4
• Molecular Formula: C₁₅H₁₅BrO
• Molecular Weight: 291.187

Synonyms:mesityl 4-bromophenyl ether

Chemical Property of mesityl 4-bromophenyl ether

Chemical Property:

Purity/Quality:

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Technology Process of mesityl 4-bromophenyl ether

There total 2 articles about mesityl 4-bromophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-phenol (106-41-2) + (4-methoxyphenyl)[[(4-methylphenyl)sulfonyl]oxy](2,4,6-trimethylphenyl)-λ3-iodane → para-iodoanisole (696-62-8) + mesityl 4-bromophenyl ether (118095-18-4)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 168h; Overall yield = 55 %Spectr.; Inert atmosphere;

DOI:10.1021/acs.joc.5b02728

Reference yield:

hydroxy{[(4-methylphenyl)sulfonyl]oxy}-(2,4,6-trimethylphenyl)-λ3–iodine → mesityl 4-bromophenyl ether (118095-18-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 168 h / 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; triethylamine; In dichloromethane;

DOI:10.1021/acs.joc.5b02728

upstream raw materials:

4-bromo-phenol

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