(SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)

Base Information

• Chemical Name: (SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)
• CAS No.: 425603-91-4
• Molecular Formula: C₈₁H₉₄N₈O₁₄Zn
• Molecular Weight: 1469.07

Synonyms:(SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)

Chemical Property of (SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)

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Technology Process of (SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)

There total 1 articles about (SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-bromo-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)](2-)-N(21),N(22),N(23),N(24)]zinc(II) (253604-41-0) + 2-{3,5-bis[6-(1H-imidazol-1-yl)hexyloxy]-4-methylphenyl}-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (253604-35-2) → (SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)](2-)-N(21),N(22),N(23),N(24)]zinc(II) (425603-91-4)

Guidance literature:

With Cs₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; toluene; suspn. of Zn-complex, ligand, Cs2CO3 and Pd-complex in toluene and THF was degassed, heated to reflux for 6 h in the dark under N2; cooled to room temp., CH2Cl2 was added, filtered, concd. in vacuo, purified by FC on SiO2 with CH2Cl2/MeOH, dried under vac., recrystd. from CHCl3/hepatne at -20°C; elem. anal.;

DOI:10.1002/1522-2675(200202)85:2<571::AID-HLCA571>3.0.CO;2-Y

Reference yield:

(SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-(3,5-bis[[6-(1H-imidazole-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)](2-)-N(21),N(22),N(23),N(24)]zinc(II) (425603-91-4) → Zn(HCO2CH2CH2CH2O)4C6H3C6H3C20H9N4(C6H2CH3(O(CH2)6C3H3N2)2) (425603-90-3)

Guidance literature:

With NaOH; In 1,4-dioxane; Zn-complex was dissolved in dioxane and NaOH was added, stirred in the dark at room temp. for 3 d; extd. with CHCl3, aq. phase was acidified with HCl, satd. with NaCl, filtered, washed with H2O, acetone, Et2O, dried under vac. in the dark for 2 h;

DOI:10.1002/1522-2675(200202)85:2<571::AID-HLCA571>3.0.CO;2-Y

upstream raw materials:

(SP-4-2)-[[tetraethyl 4,4',4'',4'''-[10-bromo-21H,23H-porphine-5,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis(butanoato)]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾]zinc(II)

2-{3,5-bis[6-(1H-imidazol-1-yl)hexyloxy]-4-methylphenyl}-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Downstream raw materials:

Zn(HCO₂CH₂CH₂CH₂O)4C₆H₃C₆H₃C₂₀H₉N₄(C₆H₂CH₃(O(CH₂)6C₃H₃N₂)2)

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