Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

Base Information

Chemical Name:Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate
CAS No.:857900-58-4
Molecular Formula:C₂₅H₃₆N₄O₄
Molecular Weight:456.585
Hs Code.:

Synonyms:Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

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Chemical Property of Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

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Technology Process of Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

There total 2 articles about Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 857904-28-0
Tert-butyl (1S,2S)-1-benzyl-3-(1-benzyl-2-{(2S,3S)-2-[(methoxycarbonyl)amino]-3-methylpentanoyl}hydrazino)-2-hydroxypropylcarbamate

: 857900-58-4
Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 70 ℃; for 3h;

Reference yield:

: (3S,4S)-3-[(methoxycarbonyl)amino]-4-methylhexanoic Acid

: 857904-18-8
Tert-butyl (1S,2S)-1-benzyl-3-(1-benzylhydrazino)-2-hydroxypropylcarbamate

: 857900-58-4
Methyl (1S,2S)-1-({2-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyl]-2-benzylhydrazino}carbonyl)-2-methylbutylcarbamate

Guidance literature:: (3S,4S)-3-[(methoxycarbonyl)amino]-4-methylhexanoic Acid; Tert-butyl (1S,2S)-1-benzyl-3-(1-benzylhydrazino)-2-hydroxypropylcarbamate; With triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 25 ℃; for 4h;

With hydrogenchloride; water; In tetrahydrofuran; at 70 ℃; for 3h;

With sodium hydrogencarbonate; In tetrahydrofuran; water; Product distribution / selectivity;