7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:165191-71-9
Molecular Formula:C₇₄H₁₃₄N₆O₁₂
Molecular Weight:1299.91
Hs Code.:

Synonyms:7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Chemical Property of 7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 10 articles about 7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₇₄H₁₂₆N₆O₁₆

: 165191-71-9
7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 72h; Inert atmosphere;
DOI:10.1055/s-0034-1378345

Reference yield: 48.0%

: 94605-71-7
7-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 165191-78-6
N,N'-di-(n-12-bromododecyl)-4,13-diaza-18-crown-6

: 165191-71-9
7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium carbonate; potassium iodide; In various solvent(s); for 24h; Heating;
DOI:10.1021/ja00134a011

Reference yield:

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 165191-71-9
7,16-bis-[12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadec-7-yl)-dodecyl]-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / Na₂CO₃, KI / various solvent(s) / 24 h / Heating

2: 48 percent / Na₂CO₃, KI / various solvent(s) / 24 h / Heating

With sodium carbonate; potassium iodide; In various solvent(s);
DOI:10.1021/ja00134a011