{2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine

Base Information

• Chemical Name: {2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine
• CAS No.: 252664-92-9
• Molecular Formula: C₂₈H₂₇ClN₈O₃
• Molecular Weight: 559.027

Synonyms:{2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine

Chemical Property of {2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine

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Technology Process of {2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine

There total 1 articles about {2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3AS,4S,6R,6AR)-6-[2-Chloro-6-(2,2-diphenyl-ethylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid hydrazide (252664-90-7) + ethyl formimidate hydrochloride (16694-46-5) → {2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine (252664-92-9)

Guidance literature:

With triethylamine; In ethanol; for 68h; Heating / reflux;

Reference yield:

{2-chloro-9-[6R-(4H-[1,2,4]triazol-3-yl)-2,2-dimethyltetrahydro-(3aR,6aR)-furo[3,4-d][1,3]dioxol-4R-yl]-9H-purin-6-yl}-(2,2-diphenylethyl)amine (252664-92-9) + acetic acid (64-19-7,77671-22-8) → (2R,3R,4S,5R)-2-[2-chloro-6-(2,2-diphenylethylamino)purin-9-yl]-5-(4H-[1,2,4]triazol-3-yl)-tetrahydrofuran-3,4-diol acetate

Guidance literature:

With water; at 100 ℃; for 3h;

upstream raw materials:

(3AS,4S,6R,6AR)-6-[2-Chloro-6-(2,2-diphenyl-ethylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid hydrazide

ethyl formimidate hydrochloride

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