2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene

Base Information

• Chemical Name: 2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene
• CAS No.: 126972-46-1
• Molecular Formula: C₂₄H₂₀N₄P₂Se₂
• Molecular Weight: 584.317

Synonyms:2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene

Chemical Property of 2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene

Chemical Property:

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Technology Process of 2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene

There total 3 articles about 2,2,5,5-Tetraphenyl-3aλ⁴,6aλ⁴-diselena-1,3,4,6-tetraaza-2λ⁵,5λ⁵-diphospha-pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

phenylselenium trichloride (42572-42-9) + Ph2P(=NSiMe3){N(SiMe3)2} (61500-31-0) → 2,2,5,5-Tetraphenyl-3aλ4,6aλ4-diselena-1,3,4,6-tetraaza-2λ5,5λ5-diphospha-pentalene (126972-46-1) + (1Z,4Z)-1,3,3,5,7,7-Hexaphenyl-1λ4,5λ4,3λ5,7λ5-[1,5,2,4,6,8,3,7]diselenatetrazadiphosphocine (126972-43-8,130010-87-6)

Guidance literature:

In acetonitrile; at 23 ℃;

DOI:10.1039/c39890001703

Reference yield: 85.0%

Ph2P(=NSiMe3){N(SiMe3)2} (61500-31-0) → 2,2,5,5-Tetraphenyl-3aλ4,6aλ4-diselena-1,3,4,6-tetraaza-2λ5,5λ5-diphospha-pentalene (126972-46-1)

Guidance literature:

With selenium tetrachloride; diselenium dichloride; In acetonitrile; at 23 ℃; for 16h;

DOI:10.1039/c39920001330

Reference yield: 50.0%

C2H5Cl3Se (37773-45-8) + Ph2P(=NSiMe3){N(SiMe3)2} (61500-31-0) → 2,2,5,5-Tetraphenyl-3aλ4,6aλ4-diselena-1,3,4,6-tetraaza-2λ5,5λ5-diphospha-pentalene (126972-46-1) + (1Z,4Z)-1,5-Diethyl-3,3,7,7-tetraphenyl-1λ4,5λ4,3λ5,7λ5-[1,5,2,4,6,8,3,7]diselenatetrazadiphosphocine (126972-45-0)

Guidance literature:

In acetonitrile; at 23 ℃;

DOI:10.1039/c39890001703

upstream raw materials:

C₂H₅Cl₃Se

Ph₂P(=NSiMe₃){N(SiMe₃)2}

phenylselenium trichloride

Downstream raw materials:

Pd(P(C₆H₅)3)2(Se₂N₄P₂(C₆H₅)4)

PtCl₂(P(C₂H₅)3)Se(NP(C₆H₅)2N)Se(NP(C₆H₅)2N)Pt(P(C₆H₅)3)2

(PtCl₂(P(C₂H₅)3))2(Se₂N₄P₂(C₆H₅)4)

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