(5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

Base Information

Chemical Name:(5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether
CAS No.:85304-90-1
Molecular Formula:C₁₅H₂₆O
Molecular Weight:222.371
Hs Code.:

Synonyms:(5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

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Chemical Property of (5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

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Technology Process of (5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

There total 2 articles about (5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 85304-99-0
(5'-tert-butyl-1'-cyclohexenyl)methyl propionate

: 85304-90-1
(5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

Guidance literature:: In tetrahydrofuran; 1.) -40 deg C, 1 h, 2.) room temp., 1.5 h;
DOI:10.1021/jo00159a008

Reference yield:

: 62222-99-5
5-tert-butyl-1-(hydroxymethyl)-1-cyclohexene

: 85304-90-1
(5'-tert-butyl-1'-cyclohexyl)methyl buten-2-yl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) room temp., 1 h

2: 86 percent / tetrahydrofuran / 1.) -40 deg C, 1 h, 2.) room temp., 1.5 h

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00159a008