C₂₇H₂₄N₆O₁₅S₄

Base Information

• Chemical Name: C₂₇H₂₄N₆O₁₅S₄
• CAS No.: 1516880-76-4
• Molecular Formula: C₂₇H₂₄N₆O₁₅S₄
• Molecular Weight: 800.783
• Mol file: 1516880-76-4.mol

Synonyms:C₂₇H₂₄N₆O₁₅S₄

Chemical Property of C₂₇H₂₄N₆O₁₅S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₄N₆O₁₅S₄

There total 2 articles about C₂₇H₂₄N₆O₁₅S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(p-aminophenylsulfonyl)ethyl hydrogen sulfate (2494-89-5) + C19H16N4O9S2 (1516880-75-3) → C27H24N6O15S4 (1516880-76-4)

Guidance literature:

2-(p-aminophenylsulfonyl)ethyl hydrogen sulfate; With hydrogenchloride; In water; at 0 - 5 ℃; for 0.166667h;

With aminosulfonic acid; sodium nitrite; In water; at 0 - 5 ℃; for 1h;

C₁₉H₁₆N₄O₉S₂; In water; for 2h;

Reference yield:

4-amino-5-hydroxy-2,7-naphthalenedisulfonic acid (90-20-0) + 3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridone (28141-13-1) → C27H24N6O15S4 (1516880-76-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium nitrite / water / 0.17 h / 0 - 5 °C

1.2: 0.5 h / 0 - 5 °C

1.3: 0 - 5 °C

2.1: hydrogenchloride / water / 0.17 h / 0 - 5 °C

2.2: 1 h / 0 - 5 °C

2.3: 2 h

With hydrogenchloride; sodium nitrite; In water;

upstream raw materials:

4-amino-5-hydroxy-2,7-naphthalenedisulfonic acid

3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridone

2-(p-aminophenylsulfonyl)ethyl hydrogen sulfate

C₁₉H₁₆N₄O₉S₂

Refernces