2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

Base Information

Chemical Name:2,4,6-Trimethylbenzyl 12-hydroxydodecanoate
CAS No.:153959-38-7
Molecular Formula:C₂₂H₃₆O₃
Molecular Weight:348.526
Hs Code.:

Synonyms:2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

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Chemical Property of 2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

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Technology Process of 2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

There total 1 articles about 2,4,6-Trimethylbenzyl 12-hydroxydodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 505-95-3
12-hydroxydodecanoic acid

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 153959-38-7
2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

Guidance literature:: With triethylamine; In ethyl acetate; for 12h; Heating;
DOI:10.1021/jo00082a009

Reference yield: 60.6%

: 107033-46-5
(R)-(tert-butyldiphenylsilyloxy)methyloxirane

: 153959-38-7
2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

: 12-[2-(tert-Butyl-diphenyl-silanyloxy)-1-hydroxymethyl-ethoxy]-dodecanoic acid 2,4,6-trimethyl-benzyl ester

: 153959-39-8
1-O-<11-<<(2,4,6-Trimethylbenzyl)oxy>carbonyl>undecyl>-3-O-(tert-butyldiphenylsilyl)-sn-glycerol

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; Ambient temperature;
DOI:10.1021/jo00082a009

Reference yield:

: 153959-38-7
2,4,6-Trimethylbenzyl 12-hydroxydodecanoate

: 1027910-75-3
12-[(R)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methoxy-propoxy]-dodecanoic acid 2,4,6-trimethyl-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60.6 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

2: NaH / hexane; tetrahydrofuran / 28 h

With boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/jo00082a009