Technology Process of C36H38O4
There total 8 articles about C36H38O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: boron tribromide / dichloromethane / 2 h / -78 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / Cooling with ice
3.1: potassium hydroxide / ethanol / 1.5 h / 55 °C
4.1: iodine; pyridine / Reflux
5.1: hydrogenchloride / dichloromethane; isopropyl alcohol
6.1: sodium hydride / dichloromethane; isopropyl alcohol / 2 h / 20 °C / Inert atmosphere
7.1: palladium 10% on activated carbon; hydrogen / ethyl acetate
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; iodine; boron tribromide; sodium hydride; N-ethyl-N,N-diisopropylamine; potassium hydroxide;
In
ethanol; dichloromethane; ethyl acetate; isopropyl alcohol;
3.1: |Claisen-Schmidt Condensation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: iodine; pyridine / Reflux
2: hydrogenchloride / dichloromethane; isopropyl alcohol
3: sodium hydride / dichloromethane; isopropyl alcohol / 2 h / 20 °C / Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / ethyl acetate
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; iodine; sodium hydride;
In
dichloromethane; ethyl acetate; isopropyl alcohol;