[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Base Information

Chemical Name:[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose
CAS No.:1315205-76-5
Molecular Formula:C₆₉H₇₈O₁₇
Molecular Weight:1179.37
Hs Code.:

Synonyms:[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Suppliers and Price of [2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

There total 4 articles about [2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1315206-12-2
(3R,4S,5S,6S)-6-hydroxy-4,5-bis(4-methoxybenzyloxy)-2-((4-methoxybenzyloxy)methyl)octa-1,7-dien-3-yl 2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranoside

: 1315205-76-5
[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: C₇₆H₈₁NO₂₀

: 1315205-76-5
[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Guidance literature:: With sodium hydroxide; In methanol; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: 1315205-72-1
(3R,4S,5R)-4,5-bis(4-methoxybenzyloxy)-2-((4-methoxybenzyloxy)methyl)-6-oxohex-1-en-3-yl 2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranoside

: 1315205-76-5
[2,3,4,6-O-tetrakis-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-(1->4)-α-2,3,6-tris-O-(4-methoxyphenylmethyl)-Δ(5,5a)carbaglucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.17 h / -15 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 0.17 h / 80 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2011.04.048