C₄₃H₆₀O₈

Base Information

Chemical Name:C₄₃H₆₀O₈
CAS No.:954106-26-4
Molecular Formula:C₄₃H₆₀O₈
Molecular Weight:704.945
Hs Code.:

C<sub>43</sub>H<sub>60</sub>O<sub>8</sub>

Synonyms:C₄₃H₆₀O₈

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Chemical Property of C₄₃H₆₀O₈

Chemical Property:

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Technology Process of C₄₃H₆₀O₈

There total 14 articles about C₄₃H₆₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 954106-39-9
C₂₅H₃₁NO₄

: 954106-26-4
C₄₃H₆₀O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaHDMS / tetrahydrofuran / 2 h / -78 °C

1.2: 80 percent / tetrahydrofuran / -78 - -20 °C

2.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

3.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

4.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

5.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

5.2: Me₃SiCl / 0.58 h / -78 - 0 °C

6.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

With dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide; 5.1: Ireland-Claisen rearrngement;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-40-2
C₂₇H₃₆O₅

: 954106-26-4
C₄₃H₆₀O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

2.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

3.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

3.2: Me₃SiCl / 0.58 h / -78 - 0 °C

4.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

With dmap; lithium aluminium tetrahydride; n-butyllithium; hydrogen; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide; 3.1: Ireland-Claisen rearrngement;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-23-1
C₃₇H₄₅NO₆

: 954106-26-4
C₄₃H₆₀O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

2.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

3.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

4.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

4.2: Me₃SiCl / 0.58 h / -78 - 0 °C

5.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

With dmap; lithium hydroxide; lithium aluminium tetrahydride; n-butyllithium; hydrogen; dihydrogen peroxide; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide; 4.1: Ireland-Claisen rearrngement;
DOI:10.1016/j.tetlet.2007.07.182